(1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide

Base Information

• Chemical Name: (1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide
• CAS No.: 1370729-77-3
• Molecular Formula: C₂HF₆NO₄S₂*C₄₀H₄₀N₆
• Molecular Weight: 885.954

Synonyms:(1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide

Chemical Property of (1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide

Chemical Property:

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Technology Process of (1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide

There total 4 articles about (1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dichloroquinoline (703-61-7) → (1R,2R)-1,2-diphenyl-N1,N2-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide (1370729-77-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate / toluene / 2 h / 80 °C / Inert atmosphere

2: α,α,α-trifluorotoluene / 0.17 h / 170 °C / Microwave irradiation

3: dichloromethane / 0.5 h / 0 - 20 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In dichloromethane; α,α,α-trifluorotoluene; toluene;

DOI:10.1021/ja301858r

Reference yield:

(R,R)-1,2-diphenylethylenediamine (35132-20-8) → (1R,2R)-1,2-diphenyl-N1,N2-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide (1370729-77-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate / toluene / 2 h / 80 °C / Inert atmosphere

2: α,α,α-trifluorotoluene / 0.17 h / 170 °C / Microwave irradiation

3: dichloromethane / 0.5 h / 0 - 20 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In dichloromethane; α,α,α-trifluorotoluene; toluene;

DOI:10.1021/ja301858r

Reference yield:

(1R,2R)-1,2-diphenyl-N1,N2-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine (1370729-76-2) + bis(trifluoromethanesulfonyl)amide (82113-65-3) → (1R,2R)-1,2-diphenyl-N1,N2-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine bistrifluoromethanesulfonimide (1370729-77-3)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 0.5h;

DOI:10.1021/ja301858r

upstream raw materials:

(1R,2R)-N₁,N₂-bis(4-chloroquinolin-2-yl)-1,2-diphenylethane-1,2-diamine

(1R,2R)-1,2-diphenyl-N₁,N₂-bis(4-(pyrrolidin-1-yl)quinolin-2-yl)ethane-1,2-diamine

bis(trifluoromethanesulfonyl)amide

(R,R)-1,2-diphenylethylenediamine

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