Boc-protected (α)N-benzyl-aeg methyl ester

Base Information

Chemical Name:Boc-protected (α)N-benzyl-aeg methyl ester
CAS No.:1430739-37-9
Molecular Formula:C₁₇H₂₆N₂O₄
Molecular Weight:322.404
Hs Code.:

Synonyms:Boc-protected (α)N-benzyl-aeg methyl ester

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Chemical Property of Boc-protected (α)N-benzyl-aeg methyl ester

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Technology Process of Boc-protected (α)N-benzyl-aeg methyl ester

There total 2 articles about Boc-protected (α)N-benzyl-aeg methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128421-86-3
methyl N-(2-(tert-butyloxycarbonyl)aminoethyl)glycinate

: 100-39-0
benzyl bromide

: 1430739-37-9
Boc-protected (α)N-benzyl-aeg methyl ester

Guidance literature:: methyl N-(2-(tert-butyloxycarbonyl)aminoethyl)glycinate; With triethylamine; In acetonitrile; at 20 ℃; for 0.25h; Inert atmosphere;

benzyl bromide; In acetonitrile; at 81 ℃;
DOI:10.1002/cplu.201300343

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1430739-37-9
Boc-protected (α)N-benzyl-aeg methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: KF celite / acetonitrile

2.1: triethylamine / acetonitrile / 0.25 h / 20 °C / Inert atmosphere

2.2: 81 °C

With triethylamine; In acetonitrile;
DOI:10.1002/cplu.201300343

Reference yield: 73.0%

: 1430739-37-9
Boc-protected (α)N-benzyl-aeg methyl ester

: 13754-41-1
4-benzyl-piperazin-2-one

Guidance literature:: Boc-protected (α)N-benzyl-aeg methyl ester; With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; for 1h; Cooling with ice;

at 110 ℃; Inert atmosphere;
DOI:10.1002/cplu.201300343