N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide

Base Information

• Chemical Name: N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide
• CAS No.: 36289-79-9
• Molecular Formula: C18H18 N4 O2
• Molecular Weight: 322.367
• Hs Code.: 2928000090
• NSC Number: 631503,87858
• Mol file: 36289-79-9.mol

Synonyms:36289-79-9;N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide;N-[(E)-[(3E)-3-(benzoylhydrazinylidene)butan-2-ylidene]amino]benzamide;NSC631503;2 3-BUTANEDIONE BIS(BENZOYLHYDRAZONE);2,3-Butanedione bis-(benzoylhydrazone);NSC87858;NSC-87858;AKOS024376389;NSC-631503;N-[(E)-[(2E)-2-(benzoylhydrazono)-1-methyl-propylidene]amino]benzamide

Chemical Property of N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 82.92000
• Density: 1.16g/cm³
• LogP: 3.38000
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 322.14297583
• Heavy Atom Count: 24
• Complexity: 455

Purity/Quality:

99% ^*data from raw suppliers

2 3-BUTANEDIONE BIS(BENZOYLHYDRAZONE) 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC(=O)C1=CC=CC=C1)C(=NNC(=O)C2=CC=CC=C2)C
• Isomeric SMILES: C/C(=N\NC(=O)C1=CC=CC=C1)/C(=N/NC(=O)C2=CC=CC=C2)/C

Technology Process of N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide

There total 7 articles about N'-(2-(Benzoylhydrazono)-1-methylpropylidene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) → biacetyl bis(benzoylhydrazone) (36289-79-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol; H₂O / Heating

2: ethanol; H₂O

With hydrazine hydrate; In ethanol; water;

Reference yield:

benzoic acid hydrazide (613-94-5) + dimethylglyoxal (431-03-8) → butane-2,3-dione bis(benzoylhydrazone) (36289-79-9)

Guidance literature:

With ethanol; at 100 ℃; im Druckrohr;

Reference yield:

biacetyl monobenzoyl hydrazone (55590-53-9) → butane-2,3-dione bis(benzoylhydrazone) (36289-79-9)

Guidance literature:

With acetic acid;

upstream raw materials:

biacetyl monobenzoyl hydrazone

benzoic acid hydrazide

dimethylglyoxal

acetic acid

Downstream raw materials:

benzoic N-(4,5-dimethyl-[1,2,3]triazol-1-yl)-benzimidic anhydride

{Ni(C₆H₅CONNC(CH₃)C(CH₃)NNCOC₆H₅)}

Pd₂((C(CH₃)NNC(O)C₆H₅)2)2

[biacetyl bis-α-hydroxybenzylidenehydrazone(2-)-N(1)N(1)'OO']nickel(II)