biacetyl monobenzoyl hydrazone

Base Information

• Chemical Name: biacetyl monobenzoyl hydrazone
• CAS No.: 55590-53-9
• Molecular Formula: C₁₁H₁₂N₂O₂
• Molecular Weight: 204.228

Synonyms:biacetyl monobenzoyl hydrazone

Chemical Property of biacetyl monobenzoyl hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of biacetyl monobenzoyl hydrazone

There total 1 articles about biacetyl monobenzoyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid hydrazide (613-94-5) + dimethylglyoxal (431-03-8) → biacetyl monobenzoyl hydrazone (55590-53-9)

Guidance literature:

With water;

Reference yield: 80.0%

biacetyl monobenzoyl hydrazone (55590-53-9) + N-4-chlorophenylhydrazine (1073-69-4) → C16H16Cl2N4 + biacetyl benzoylhydrazone (p-chlorophenyl)hydrazone (138815-27-7)

Guidance literature:

With acetic acid; In ethanol; water; for 0.0166667h; Yields of byproduct given; Heating;

DOI:10.1021/jo00034a013

Reference yield: 72.0%

biacetyl monobenzoyl hydrazone (55590-53-9) + phenylhydrazine (100-63-0) → Biacetyl Benzoylhydrazone Phenylhydrazone (31400-24-5) + butane-2,3-dione-bis-phenylhydrazone (2861-48-5)

Guidance literature:

With acetic acid; In ethanol; water; for 0.0166667h; Yields of byproduct given; Heating;

DOI:10.1021/jo00034a013

upstream raw materials:

benzoic acid hydrazide

dimethylglyoxal

Downstream raw materials:

5,6-dimethyl-3-phenyl-1,2,4-triazine

butane-2,3-dione bis(benzoylhydrazone)

5,6,N,N,N',N'-hexamethyl-2-phenyl-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,4,2]oxadiazaphosphole-8,8-diamine

8,8-dimethoxy-5,6-dimethyl-2-phenyl-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,4,2]oxadiazaphosphole

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