Acetamide, N,N'-(4-nitro-1,3-phenylene)bis-

Base Information

• Chemical Name: Acetamide, N,N'-(4-nitro-1,3-phenylene)bis-
• CAS No.: 119-76-6
• Molecular Formula: C10H11N3O4
• Molecular Weight: 237.215
• Hs Code.: 2924299090
• European Community (EC) Number: 204-349-1
• DSSTox Substance ID: DTXSID6059495
• Nikkaji Number: J29.485C
• Wikidata: Q81988829
• Mol file: 119-76-6.mol

Synonyms:119-76-6;N-(3-acetamido-4-nitrophenyl)acetamide;EINECS 204-349-1;Acetamide, N,N'-(4-nitro-1,3-phenylene)bis-;N,N'-(4-Nitro-1,3-phenylene)bis(acetamide);N,N/'-(4-nitro-1,3-phenylene)bis(acetamide);DTXSID6059495;SCHEMBL10790188;2,4-Di(acetylamino)-1-nitrobenzene;AKOS003889648

Chemical Property of Acetamide, N,N'-(4-nitro-1,3-phenylene)bis-

Chemical Property:

• Boiling Point: 548.9°Cat760mmHg
• Flash Point: 285.8°C
• PSA: 111.00000
• Density: 1.416g/cm³
• LogP: 3.33380
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 237.07495584
• Heavy Atom Count: 17
• Complexity: 326

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=CC(=C(C=C1)[N+](=O)[O-])NC(=O)C

Technology Process of Acetamide, N,N'-(4-nitro-1,3-phenylene)bis-

There total 4 articles about Acetamide, N,N'-(4-nitro-1,3-phenylene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,3-diacetylaminobenzene (10268-78-7) → N,N'-(4-nitro-m-phenylene)-bis-acetamide (119-76-6)

Guidance literature:

With sulfuric acid; nitric acid; at 5 - 10 ℃; for 0.25h;

DOI:10.1016/j.dyepig.2010.03.002

Reference yield:

m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) → N,N'-(4-nitro-m-phenylene)-bis-acetamide (119-76-6)

Guidance literature:

Multi-step reaction with 2 steps

2: glacial acetic acid; nitric acid

With nitric acid; acetic acid;

Reference yield:

2,4-diaminonitrobenzene (5131-58-8) + acetic acid (64-19-7,77671-22-8) → acetic acid-(3-amino-4-nitro-anilide) (66136-64-9) + N,N'-(4-nitro-m-phenylene)-bis-acetamide (119-76-6)

Guidance literature:

anschliessend mit Acetanhydrid;

DOI:10.1039/jr9300001910

upstream raw materials:

2,4-diaminonitrobenzene

acetic acid

1,3-diacetylaminobenzene

m-phenylenediamine

Downstream raw materials:

2,4-diaminonitrobenzene

5-chloro-2-nitrophenol

5-acetamido-2-methylbenzimidazole

1,2,4-triaminobenzene N¹,N²,N⁴-triacetate