1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

Base Information

Chemical Name:1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide
CAS No.:1274878-94-2
Molecular Formula:C₂₇H₂₇N₂O₃*I
Molecular Weight:554.427
Hs Code.:

Synonyms:1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

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Chemical Property of 1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

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Technology Process of 1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

There total 10 articles about 1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1274877-35-8
6-(2-morpholinoethoxy)-3-phenyl-2-(pyridin-3-yl)-1H-inden-1-one

: 74-88-4
methyl iodide

: 1274878-94-2
1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

: 4-methyl-4-(2-{[2-(1-methylpyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium diiodide

Guidance literature:: In dichloromethane; for 0.5h; Reflux;

Reference yield: 17.0%

: 4-methyl-4-(2-{[2-(1-methylpyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium diiodide

: 1274878-94-2
1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

Guidance literature:: With methanol; In dichloromethane;

Reference yield:

: 76106-72-4
6-hydroxy-3-phenylindan-1-one

: 1274878-94-2
1-methyl-3-{6-[2-(morpholin-4-yl)ethoxy]-1-oxo-3-phenyl-1H-inden-2-yl}pyridin-1-ium iodide

: 4-methyl-4-(2-{[2-(1-methylpyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium diiodide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dichloromethane / 8 h / 0 - 20 °C

2: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 2.5 h / Reflux; Irradiation by tungsten lamp

3: potassium carbonate; methanol / 2 h / 20 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2.5 h / 0 - 20 °C

5: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.33 h / 150 °C / microwave irradiation

6: dichloromethane / 0.5 h / Reflux

With pyridine; methanol; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; sodium carbonate; potassium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; dichloromethane; water;