1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole
CAS No.:1442445-62-6
Molecular Formula:C₁₉H₂₁Cl₂N₅
Molecular Weight:390.315
Hs Code.:

Synonyms:1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

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Chemical Property of 1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

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Technology Process of 1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

There total 5 articles about 1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89981-75-9
1-(2',4'-dichlorophenyl)ethylamine

: 1442445-62-6
1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: (S)-Mandelic acid / isopropyl alcohol; ethanol / 26 h / 30 - 60 °C / Resolution of racemate

1.2: 1 h / 20 °C / Resolution of racemate

2.1: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

3.1: potassium carbonate / dimethyl sulfoxide / 3 h / 125 °C

4.1: ammonium chloride; iron / ethanol; water / 1 h / 90 °C

5.1: sodium nitrite; acetic acid / 18 h / 20 °C

With (S)-Mandelic acid; iron; potassium carbonate; ammonium chloride; acetic acid; sodium nitrite; In ethanol; water; dimethyl sulfoxide; isopropyl alcohol;

Reference yield:

: 1442445-61-5
N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

: 1442445-62-6
1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: With acetic acid; sodium nitrite; at 20 ℃; for 18h;

Reference yield:

: 1442445-60-4
(R)-tert-butyl 4-(3-((R)-1-(2,4-dichlorophenyl)ethylamino)-4-nitrophenyl)-2-methylpiperazine-1-carboxylate

: 1442445-62-6
1-((R)-1-(2,4-dichlorophenyl)ethyl)-6-((R)-3-methylpiperazin-1-yl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; iron / ethanol; water / 1 h / 90 °C

2: sodium nitrite; acetic acid / 18 h / 20 °C

With iron; ammonium chloride; acetic acid; sodium nitrite; In ethanol; water;