N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

Base Information

Chemical Name:N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine
CAS No.:1442445-61-5
Molecular Formula:C₁₉H₂₄Cl₂N₄
Molecular Weight:379.332
Hs Code.:

Synonyms:N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

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Chemical Property of N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

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Technology Process of N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

There total 4 articles about N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89981-75-9
1-(2',4'-dichlorophenyl)ethylamine

: 1442445-61-5
N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: (S)-Mandelic acid / isopropyl alcohol; ethanol / 26 h / 30 - 60 °C / Resolution of racemate

1.2: 1 h / 20 °C / Resolution of racemate

2.1: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

3.1: potassium carbonate / dimethyl sulfoxide / 3 h / 125 °C

4.1: ammonium chloride; iron / ethanol; water / 1 h / 90 °C

With (S)-Mandelic acid; iron; potassium carbonate; ammonium chloride; In ethanol; water; dimethyl sulfoxide; isopropyl alcohol;

Reference yield:

: 1442445-60-4
(R)-tert-butyl 4-(3-((R)-1-(2,4-dichlorophenyl)ethylamino)-4-nitrophenyl)-2-methylpiperazine-1-carboxylate

: 1442445-61-5
N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 90 ℃; for 1h;

Reference yield:

: 133773-29-2
(R)-2,4-dichloro-α-methylbenzylamine

: 1442445-61-5
N-((R)-1-(2,4-dichlorophenyl)ethyl)-5-((R)-3-methylpiperazin-1-yl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

2: potassium carbonate / dimethyl sulfoxide / 3 h / 125 °C

3: ammonium chloride; iron / ethanol; water / 1 h / 90 °C

With iron; potassium carbonate; ammonium chloride; In ethanol; water; dimethyl sulfoxide;