C₃₇H₄₀Cl₃NO₂₀

Base Information

Chemical Name:C₃₇H₄₀Cl₃NO₂₀
CAS No.:1426099-72-0
Molecular Formula:C₃₇H₄₀Cl₃NO₂₀
Molecular Weight:925.078
Hs Code.:

C<sub>37</sub>H<sub>40</sub>Cl<sub>3</sub>NO<sub>20</sub>

Synonyms:C₃₇H₄₀Cl₃NO₂₀

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Chemical Property of C₃₇H₄₀Cl₃NO₂₀

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Technology Process of C₃₇H₄₀Cl₃NO₂₀

There total 13 articles about C₃₇H₄₀Cl₃NO₂₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426099-71-9
C₃₇H₄₂Cl₃NO₁₉

: 1426099-72-0
C₃₇H₄₀Cl₃NO₂₀

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; water; at 20 ℃; for 1.5h;
DOI:10.1021/ja4000933

Reference yield:

: 1885-14-9
phenyl chloroformate

: 1426099-72-0
C₃₇H₄₀Cl₃NO₂₀

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 2 h / -40 °C / Inert atmosphere

2: 2,6-di-tert-butyl-pyridine; 1,2-dimethoxy-4-(2-propenyl)benzene; trifluoromethylsulfonic anhydride / dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Molecular sieve

3: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -78 °C / Molecular sieve; Inert atmosphere

4: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: hydrogen; palladium 10% on activated carbon; trichloroacetic acid / methanol / 0.25 h

6: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; dichloromethane / 1.5 h / 20 °C

With pyridine; triethylsilane; dmap; 2,6-di-tert-butyl-pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; 1,2-dimethoxy-4-(2-propenyl)benzene; palladium 10% on activated carbon; hydrogen; trichloroacetic acid; In methanol; dichloromethane; water;
DOI:10.1021/ja4000933

Reference yield:

: 176299-96-0
4-methoxyphenyl 4,6-O-benzylidene-β-D-galactopyranoside

: 1426099-72-0
C₃₇H₄₀Cl₃NO₂₀

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 2 h / -40 °C / Inert atmosphere

2: 2,6-di-tert-butyl-pyridine; 1,2-dimethoxy-4-(2-propenyl)benzene; trifluoromethylsulfonic anhydride / dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Molecular sieve

3: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -78 °C / Molecular sieve; Inert atmosphere

4: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: hydrogen; palladium 10% on activated carbon; trichloroacetic acid / methanol / 0.25 h

6: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; dichloromethane / 1.5 h / 20 °C

With pyridine; triethylsilane; dmap; 2,6-di-tert-butyl-pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; 1,2-dimethoxy-4-(2-propenyl)benzene; palladium 10% on activated carbon; hydrogen; trichloroacetic acid; In methanol; dichloromethane; water;
DOI:10.1021/ja4000933