6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine

Base Information

• Chemical Name: 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine
• CAS No.: 1127389-80-3
• Molecular Formula: C₃₄H₃₀O₄P₂
• Molecular Weight: 564.557

Synonyms:6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine

Chemical Property of 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine

There total 2 articles about 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

→ 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine (1127389-80-3)

Guidance literature:

Reference yield:

(1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylpropan-2-ol + 6-chloro-dibenzo[d,f][1,3,2]-dioxaphosphepin (16611-68-0) → 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine (1127389-80-3)

Guidance literature:

With triethylamine; In toluene; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/adsc.200800311

Reference yield: 48.0%

bis(1,5-cyclooctadiene)diiridium(I) dichloride (12112-67-3) + 6-((1R,2S)-1-(diphenylphosphino)-3-methoxy-1-phenylprop-2-yloxy)dibenzo[d,f][1,3,2]dioxaphosphepine (1127389-80-3) + lithium iodide (10377-51-2) → [((CHCHC2H4)2)IrI(P(C6H5)2CH(C6H5)CH(CH2OCH3)OP(OC6H4)2)]

Guidance literature:

In tetrahydrofuran; Ir complex reacted with ligand in THF, refluxed with LiI in acetone;

DOI:10.1021/om100955t

upstream raw materials:

6-chloro-dibenzo[d,f][1,3,2]-dioxaphosphepin

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