ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

Base Information

Chemical Name:ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate
CAS No.:134420-78-3
Molecular Formula:C₃₀H₄₁NO₆
Molecular Weight:511.659
Hs Code.:

Synonyms:ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

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Chemical Property of ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

There total 4 articles about ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 134420-73-8
ethyl N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

: 134420-78-3
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

Guidance literature:: With potassium carbonate; In 1,4-dioxane; a) 0 deg C, 15 min, b) RT, 3 h;
DOI:10.1021/jm00112a032

Reference yield:

: 134420-92-1
ethyl 6,6-diphenyl-2-hexenoate

: 134420-78-3
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / ethanol / 48 h / Heating

2: 95 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 3040 Torr

3: 95 percent / ethanol / Ambient temperature

4: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

With hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00112a032

Reference yield:

: 134420-95-4
ethyl 3-(benzylamino)-6,6-diphenylcaproate

: 134420-78-3
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 3040 Torr

2: 95 percent / ethanol / Ambient temperature

3: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

With hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00112a032