N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone
CAS No.:134420-82-9
Molecular Formula:C₂₈H₃₅NO₅
Molecular Weight:465.59
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

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Chemical Property of N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

Chemical Property:

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Technology Process of N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

There total 5 articles about N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 134420-78-3
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-6,6-diphenylcaproate

: 134420-82-9
N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

Guidance literature:: With sodium; In ethanol; benzene; for 24h; Ambient temperature;
DOI:10.1021/jm00112a032

Reference yield:

: 134420-92-1
ethyl 6,6-diphenyl-2-hexenoate

: 134420-82-9
N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / ethanol / 48 h / Heating

2: 95 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 3040 Torr

3: 95 percent / ethanol / Ambient temperature

4: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

5: 87 percent / sodium / ethanol; benzene / 24 h / Ambient temperature

With hydrogen; sodium; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; ethanol; benzene;
DOI:10.1021/jm00112a032

Reference yield:

: 134420-95-4
ethyl 3-(benzylamino)-6,6-diphenylcaproate

: 134420-82-9
N-(tert-butyloxycarbonyl)-2-(3,3-diphenylpropyl)-5-carbethoxy-4-piperidone

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 3040 Torr

2: 95 percent / ethanol / Ambient temperature

3: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

4: 87 percent / sodium / ethanol; benzene / 24 h / Ambient temperature

With hydrogen; sodium; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; ethanol; benzene;
DOI:10.1021/jm00112a032