methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

Base Information

Chemical Name:methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate
CAS No.:1373319-41-5
Molecular Formula:C₃₀H₃₄N₄O₉
Molecular Weight:594.621
Hs Code.:

Synonyms:methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

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Chemical Property of methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

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Technology Process of methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

There total 10 articles about methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1006030-92-7
methyl 3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamino)-benzoate

: 186413-90-1
6-isopropoxy-5-nitropyridine-2-carboxylic acid

: 1373319-41-5
methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

Guidance literature:: With dichlorotriphenylphosphorane; In chloroform; Reflux; Inert atmosphere;
DOI:10.1039/c2ob07125h

Reference yield:

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

: 1373319-41-5
methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 12 h / 0 °C / Reflux; Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C / Inert atmosphere

2.2: 16 h / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / Inert atmosphere

4.1: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

5.1: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

6.1: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

With thionyl chloride; tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; triphenylphosphine; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; chloroform; ethyl acetate;
DOI:10.1039/c2ob07125h

Reference yield:

: 159783-41-2
methyl 3-isopropyloxy-4-nitrobenzoate

: 1373319-41-5
methyl 3-isopropoxy-4-(3-isopropoxy-4-(6-isopropoxy-5-nitropicolinamido)benzamido)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / Inert atmosphere

2: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

3: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

4: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

With tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; dichlorotriphenylphosphorane; In methanol; chloroform; ethyl acetate;
DOI:10.1039/c2ob07125h