2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

Base Information

Chemical Name:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt
CAS No.:1278584-01-2
Molecular Formula:C₂₅H₃₀ClN₂O₇S*Na
Molecular Weight:561.031
Hs Code.:

Synonyms:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

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Chemical Property of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

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Technology Process of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

There total 6 articles about 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

: 1278584-01-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

Guidance literature:: With sodium hydroxide; In water; isopropyl alcohol; at 20 - 60 ℃;

Reference yield:

: 1205-71-6
N-(4-chlorophenyl)aniline

: 1278584-01-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium phosphate / acetonitrile / 5.5 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

3.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

3.3: pH 7 - 8

4.1: thionyl chloride / 20 °C

5.1: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

6.1: sodium hydroxide / isopropyl alcohol; water / 20 - 60 °C

With potassium phosphate; thionyl chloride; tetrabutylammomium bromide; water; sodium hydroxide; In tetrahydrofuran; water; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

: 1187857-81-3
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

: 1278584-01-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

2: sodium hydroxide / isopropyl alcohol; water / 20 - 60 °C

With sodium hydroxide; In tetrahydrofuran; water; isopropyl alcohol;