2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

Base Information

Chemical Name:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid
CAS No.:1187857-80-2
Molecular Formula:C₂₅H₃₁ClN₂O₇S
Molecular Weight:539.049
Hs Code.:

Synonyms:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

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Chemical Property of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

Chemical Property:

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Technology Process of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

There total 14 articles about 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-35-7
Tau

: 1187857-81-3
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; Cooling with ice;

Reference yield:

: 107-35-7
Tau

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

Guidance literature:: With benzotriazol-1-ol; In water; N,N-dimethyl-formamide; at 20 - 120 ℃;

Reference yield:

: 1205-71-6
N-(4-chlorophenyl)aniline

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate / acetonitrile / 5.5 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

3.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

3.3: pH 7 - 8

4.1: thionyl chloride / 20 °C

5.1: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

With potassium phosphate; thionyl chloride; tetrabutylammomium bromide; water; sodium hydroxide; In tetrahydrofuran; water; toluene; acetonitrile;