2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

Base Information

Chemical Name:2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride
CAS No.:1187857-81-3
Molecular Formula:C₂₃H₂₅Cl₂NO₄
Molecular Weight:450.362
Hs Code.:

Synonyms:2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

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Chemical Property of 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

Chemical Property:

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Technology Process of 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

There total 11 articles about 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

: 1187857-81-3
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

Guidance literature:: With thionyl chloride; at 20 ℃;

Reference yield:

: 1205-71-6
N-(4-chlorophenyl)aniline

: 1187857-81-3
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium phosphate / acetonitrile / 5.5 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

3.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

3.3: pH 7 - 8

4.1: thionyl chloride / 20 °C

With potassium phosphate; thionyl chloride; tetrabutylammomium bromide; water; sodium hydroxide; In toluene; acetonitrile;

Reference yield:

: 1187857-74-4
N-(4-chlorophenyl)-N-phenyl-1H-imidazole-1-carboxamide

: 1187857-81-3
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

2.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

2.3: pH 7 - 8

3.1: thionyl chloride / 20 °C

With thionyl chloride; tetrabutylammomium bromide; water; sodium hydroxide; In toluene; acetonitrile;