N-Methyl-7H-dibenzo(c,g)carbazole

Base Information

• Chemical Name: N-Methyl-7H-dibenzo(c,g)carbazole
• CAS No.: 27093-62-5
• Molecular Formula: C₂₁H₁₅N
• Molecular Weight: 281.357
• Hs Code.: 2933990090
• UNII: CW2LR35YB3
• DSSTox Substance ID: DTXSID70181557
• Nikkaji Number: J34.860K
• Wikidata: Q26840997
• Mol file: 27093-62-5.mol

Synonyms:7-Me-DBC;7-methyldibenzo(c,g)carbazole;N-MeDBC;N-methyl-7H-dibenzo(c,g)carbazole

Chemical Property of N-Methyl-7H-dibenzo(c,g)carbazole

Chemical Property:

• Vapor Pressure: 3.84E-11mmHg at 25°C
• Refractive Index: 1.8240 (estimate)
• Boiling Point: 525.7°Cat760mmHg
• Flash Point: 271.7°C
• PSA: 4.93000
• Density: 1.18g/cm³
• LogP: 5.63790
• XLogP3: 5.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 281.120449483
• Heavy Atom Count: 22
• Complexity: 380

Purity/Quality:

99% ^*data from raw suppliers

7-Methyl-7H-dibenzo[c,g]carbazole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C2=C(C3=CC=CC=C3C=C2)C4=C1C=CC5=CC=CC=C54

Technology Process of N-Methyl-7H-dibenzo(c,g)carbazole

There total 3 articles about N-Methyl-7H-dibenzo(c,g)carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

7H-dibenzo[c,g]carbazole (194-59-2) + methyl iodide (74-88-4) → N-methyl-7H-dibenzo[c,g]carbazole (27093-62-5)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 2 h; 2.) -78 deg C -> room temp.;

Reference yield:

methylamine (74-89-5) + 1,1'-bi-2-naphthol (602-09-5) → N-methyl-7H-dibenzo[c,g]carbazole (27093-62-5)

Guidance literature:

at 260 ℃;

Reference yield:

→ N-methyl-7H-dibenzo[c,g]carbazole (27093-62-5)

Guidance literature:

durch Dehydrierung von 7 mit Chloranil;

upstream raw materials:

methylamine

1,1'-bi-2-naphthol

7H-dibenzo[c,g]carbazole

methyl iodide