3-dimesitylborylbenzaldehyde

Base Information

Chemical Name:3-dimesitylborylbenzaldehyde
CAS No.:1567979-48-9
Molecular Formula:C₂₅H₂₇BO
Molecular Weight:354.3
Hs Code.:

Synonyms:3-dimesitylborylbenzaldehyde

Suppliers and Price of 3-dimesitylborylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-dimesitylborylbenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-dimesitylborylbenzaldehyde

There total 3 articles about 3-dimesitylborylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 436-59-9
dimesitylfluoroborane

: 75148-49-1
3-bromobenzaldehyde diethylacetal

: 1567979-48-9
3-dimesitylborylbenzaldehyde

Guidance literature:: 3-bromobenzaldehyde diethylacetal; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

dimesitylfluoroborane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In tetrahydrofuran; hexane; water; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3dt52565a

Reference yield: 64.0%

: 150990-60-6
3-(diethoxymethyl)benzaldehyde

: 436-59-9
dimesitylfluoroborane

: 1567979-48-9
3-dimesitylborylbenzaldehyde

Guidance literature:: 3-(diethoxymethyl)benzaldehyde; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere; Schlenk technique;

dimesitylfluoroborane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic402470a

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 1567979-48-9
3-dimesitylborylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / ethanol; water / 4 h / Inert atmosphere; Schlenk technique; Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: 12 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.3: 4 h / 20 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; ethanol; hexane; water;
DOI:10.1039/c3dt52565a