3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

Base Information

Chemical Name:3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene
CAS No.:1354013-72-1
Molecular Formula:C₁₉H₁₅BF₂I₃N₃O₂
Molecular Weight:746.868
Hs Code.:

Synonyms:3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

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Chemical Property of 3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

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Technology Process of 3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

There total 2 articles about 3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1354013-80-1
4,4-difluoro-2,3,5,6-tetraiodo-8-(4-methylphenyl)-4-bora-3a,4a-diaza-s-indacene

: 107-95-9
3-amino propanoic acid

: 1354013-72-1
3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

Guidance literature:: In acetonitrile; for 4h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.070

Reference yield:

: 955084-10-3
5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1354013-72-1
3-(2-carboxyethylamino)-4,4-difluoro-2,5,6-triiodo-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

Guidance literature:: Multi-step reaction with 2 steps

1: Iodine monochloride / methanol; dichloromethane / 6 h / Reflux

2: acetonitrile / 4 h / Reflux; Inert atmosphere

With Iodine monochloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.11.070