Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4

Base Information

• Chemical Name: Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4
• CAS No.: 1020182-78-8
• Molecular Formula: C₅₉H₉₄I₂O₁₀P₄Pt₂
• Molecular Weight: 1731.25

Synonyms:Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4

Chemical Property of Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4

Chemical Property:

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Technology Process of Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4

There total 1 articles about Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

trans diiodobis(triethylphosphine)platinum(II) (35084-99-2,15692-97-4,15636-79-0) + 3,5-diethynylphenol dibenzo[24]crown-8-carboxylate (1020182-77-7) → Pt2I2(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4 (1020182-78-8)

Guidance literature:

With copper(l) iodide; In toluene; byproducts: (CH3CH2)2NH2I; addn. of toluene and amine deriv. to mixt. of platinum compd. and crown ether deriv. under N2, stirring at room temp. for 10 min, addn. of copper compd., keeping at room temp. for 16 h; evapn., chromy. (silica gel, CH2Cl2/acetone (5:1)), elem. anal.;

DOI:10.1021/ja711502t

Reference yield: 90.0%

Pt2I2(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4 (1020182-78-8) + silver trifluoromethanesulfonate (2923-28-6) → (3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(Pt(triethylphosphine)2(triflate))2 (1020182-79-9)

Guidance literature:

In dichloromethane; byproducts: AgI; addn. of silver triflate to CH2Cl2 soln. of platinum compd., keeping for4 h at room temp.; filtration, concg., addn. of diethyl ether, isolation of ppt., elem. anal.;

DOI:10.1021/ja711502t

upstream raw materials:

trans diiodobis(triethylphosphine)platinum(II)

3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

Downstream raw materials:

(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(Pt(triethylphosphine)2(triflate))2

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