3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

Base Information

Chemical Name:3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose
CAS No.:171502-63-9
Molecular Formula:C₃₁H₄₄O₈S
Molecular Weight:576.752
Hs Code.:

Synonyms:3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

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Technology Process of 3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

There total 1 articles about 3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 22529-61-9
(1R)-1-((3aR,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro(2,3-d)(1,3)dioxol-5-yl)ethane-1,2-diol

: 171502-63-9
3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: With pyridine; at 0 ℃;
DOI:10.1016/0957-4166(95)00218-E

Reference yield: 93.0%

: 64-18-6
formic acid

: 171502-63-9
3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

: 3-O-benzyl-5-O-formyl-1,2-O-isopropylidene-6-O-(2,4,6-triisopropylbenzenesulfonyl)-α-D-glucofuranose

Guidance literature:: With pyridine; acetic anhydride; at 0 ℃; for 3h;
DOI:10.1080/10426500307948

Reference yield:

: 171502-63-9
3-O-benzyl-6-O-(triisopropylbenzenesulfonyl)-1,2-O-isopropylidene-α-D-glucofuranose

: (Z)-3-O-benzyl-1,2-O-isopropylidene-6-O-(2,4,6-triisopropylbenzenesulfonyl)-5-O-(2'-trimethylsilyl-vinyl)-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine; Ac₂O / 3 h / 0 °C

2: toluene / 3 h / 110 °C

With pyridine; acetic anhydride; In toluene;
DOI:10.1080/10426500307948