2,3,3-Triphenylprop-2-enoic acid

Base Information

Chemical Name:2,3,3-Triphenylprop-2-enoic acid
CAS No.:4452-05-5
Molecular Formula:C21H16O2
Molecular Weight:300.357
Hs Code.:
NSC Number:84279
DSSTox Substance ID:DTXSID90292634

Synonyms:4452-05-5;Triphenylacrylsaure;2,3,3-triphenylprop-2-enoic acid;NSC84279;SCHEMBL2908978;DTXSID90292634;NSC-84279

Suppliers and Price of 2,3,3-Triphenylprop-2-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,3,3-Triphenylprop-2-enoic acid

Chemical Property:

Vapor Pressure:7.92E-07mmHg at 25°C
Boiling Point:391.4°C at 760 mmHg
Flash Point:289.2°C
Density:1.184g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:300.115029749
Heavy Atom Count:23
Complexity:399

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=C(C2=CC=CC=C2)C(=O)O)C3=CC=CC=C3

Technology Process of 2,3,3-Triphenylprop-2-enoic acid

There total 22 articles about 2,3,3-Triphenylprop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 119-61-9
benzophenone

: 59176-55-5
ethyl α,α-dibromobenzeneacetate

: 4452-05-5
2,3,3-triphenylacrylic acid

Guidance literature:: ethyl α,α-dibromobenzeneacetate; With naphthalene; lithium; In tetrahydrofuran; at -78 - 20 ℃;

benzophenone; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo0497813

Reference yield: 71.0%

: 6304-33-2
2,3,3-triphenylacrylonitrile

: 4452-05-5
2,3,3-triphenylacrylic acid

Guidance literature:: 2,3,3-triphenylacrylonitrile; With potassium hydroxide; In water; ethylene glycol; at 185 ℃; for 48h;

With hydrogenchloride; In water; ethylene glycol; at 20 ℃; pH=5 - 6;
DOI:10.1039/c3ra23188g

Reference yield: 64.0%

: 124-38-9,18923-20-1
carbon dioxide

: 100-58-3
phenylmagnesium bromide

: 501-65-5
diphenyl acetylene

: 4452-05-5
2,3,3-triphenylacrylic acid

Guidance literature:: phenylmagnesium bromide; diphenyl acetylene; With nickel dichloride; In tetrahydrofuran; toluene; at 60 ℃; for 2h; Schlenk technique; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; toluene; at 20 ℃; for 0.5h; under 760.051 Torr; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01693