N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

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Chemical Name:N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine
CAS No.:1169709-84-5
Molecular Formula:C₂₉H₃₅N₃Si
Molecular Weight:453.702
Hs Code.:

Synonyms:N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

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Chemical Property of N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

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Technology Process of N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

There total 1 articles about N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 75-77-4
chloro-trimethyl-silane

: 3333-52-6
2,2,3,3-tetramethylsuccinonitrile

: 36809-26-4
4-N,N-diphenylamino-1-bromobenzene

: 1169709-84-5
N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

Guidance literature:: 2,2,3,3-tetramethylsuccinonitrile; 4-N,N-diphenylamino-1-bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 2h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 0 ℃;
DOI:10.1002/ejoc.200900045

Reference yield: 52.0%

: 92-66-0
4-bromo-1,1'-biphenyl

: 1169709-84-5
N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

: N-{5-[-(4-diphenylamino)phenyl]-3,3,4,4-tetramethyl-3,4-dihydropyrrol-2-ylidene}-4-phenylbenzeneamine

Guidance literature:: With potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium dichloride; In toluene; for 6h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200900045

Reference yield: 36.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 1169709-84-5
N-phenyl-N-{4-[3,3,4,4-tetramethyl-5-(trimethylsilylimino)-4,5-dihydro-3H-pyrrol-2-yl]phenyl}benzeneamine

: N-{5-[-(4-diphenylamino)phenyl]-3,3,4,4-tetramethyl-3,4-dihydropyrrol-2-ylidene}-2,4,6-trimethylbenzeneamine

Guidance literature:: With potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium dichloride; In toluene; for 6h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200900045