S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Base Information

Chemical Name:S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate
CAS No.:238752-68-6
Molecular Formula:C₂₉H₃₆O₅S₂
Molecular Weight:528.734
Hs Code.:

Synonyms:S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Suppliers and Price of S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

There total 7 articles about S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 507-09-5
tiolacetic acid

: 238752-67-5
3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>-1-propanol

: 238752-68-6
S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1.) 0 deg C, 1 h, 2.) 0 deg C to r.t., 17 h;
DOI:10.1055/s-1999-3498

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 238752-68-6
S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / K₂CO₃ / dimethylformamide / 20 h / 60 °C

2: 64 percent / KOH / methanol / 6 h / Heating

3: 69 percent / K₂CO₃ / dimethylformamide / 24 h / 75 °C

4: 1.) 9-BBN, 2.) H₂O₂, H₂O, KOH / 1.) THF, reflux, 6 h, 2.) THF, 50 deg C, 1.5 h; 15 h

5: 79 percent / PPh₃, DEAD / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) 0 deg C to r.t., 17 h

With potassium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; water; dihydrogen peroxide; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3498

Reference yield:

: 6411-34-3
4-allyloxyphenol

: 238752-68-6
S-3-<4-(4-<4-<4-(2-Thienyl)butoxy>phenoxy>butoxy)phenoxy>propyl thioacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / KOH / methanol / 6 h / Heating

2: 69 percent / K₂CO₃ / dimethylformamide / 24 h / 75 °C

3: 1.) 9-BBN, 2.) H₂O₂, H₂O, KOH / 1.) THF, reflux, 6 h, 2.) THF, 50 deg C, 1.5 h; 15 h

4: 79 percent / PPh₃, DEAD / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) 0 deg C to r.t., 17 h

With potassium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; water; dihydrogen peroxide; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3498