[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

Base Information

Chemical Name:[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]
CAS No.:1025455-41-7
Molecular Formula:C₇₂H₁₀₀OP₂PtSSi₇
Molecular Weight:1467.28
Hs Code.:

Synonyms:[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

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Chemical Property of [(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

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Technology Process of [(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

There total 1 articles about [(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 135139-68-3
(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SH)(OH)

: 1025455-41-7
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

Guidance literature:: With sodium hydride; In tetrahydrofuran; treatment of (C6H2(CH(SiMe3)2)3)(Mes)Si(OH)(SH) with 2 molar equiv. of NaH at 0°C; addn. of THF soln. of cis-PtCl2(PPh3)2 at 0°C; warming to room temp.;
DOI:10.1021/om800210g

Reference yield: 79.0%

: 1025455-41-7
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

: lithium chloride

: 1025455-47-3
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(OH)Cl(μ-S)Pt(triphenylphosphine)2(mesityl)]

Guidance literature:: With acetic acid; In tetrahydrofuran; treatment of (C6H2((SiMe3)2CH)3)Si(μ-O)(μ-S)Pt(PPh3)2(Mes) with 1 molar equiv. of acetic acid; addn. of 1 equiv. LiCl;
DOI:10.1021/om800210g

Reference yield: 68.0%

: 1025455-41-7
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-S)Pt(triphenylphosphine)2]

: 7732-18-5
water

: 1025455-53-1
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(OH)2(μ-Se)Pt(triphenylphosphine)2(mesityl)]

Guidance literature:: With hydrogenchloride; In diethyl ether; treatment of (C6H2((SiMe3)2CH)3)(Mes)Si(μ-O)(μ-Se)Pt(PPh3)2 with 1molar equiv. of anhyd. HCl (Et2O soln.); addn. of excess of H2O;
DOI:10.1021/om800210g