((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

Base Information

Chemical Name:((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate
CAS No.:1137726-90-9
Molecular Formula:C₁₈H₂₄N₄O₅
Molecular Weight:376.412
Hs Code.:

Synonyms:((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

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Technology Process of ((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

There total 1 articles about ((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1137726-92-1
tert-butyl (3aR,4S,7aS)-3-acetyl-2-oxo-2,3,3a,4,5,7a-hexahydrobenzo[d]oxazol-4-ylcarbamate

: 6625-70-3
acetoxymalononitrile

: 1137726-90-9
((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis(diphenylphosphino)ferrocene; In toluene; at 60 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.200804777

Reference yield: 58.0%

: 1137726-90-9
((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

: 1184177-10-3
C₁₈H₂₃ClN₄O₅

Guidance literature:: With trichloroisocyanuric acid; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1016/j.tet.2009.05.077

Reference yield:

: 64-17-5
ethanol

: 1137726-90-9
((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate

: 1184177-04-5
ethyl (3S,4R,5S)-4-acetamido-5-(tert-butoxycarbonylamino)-3-hydroxycyclohex-1-enecarboxylate

Guidance literature:: ((1S,4S,5S)-4-acetamido-5-(tert-butoxycarbonylamino)cyclohex-2-enyl)dicyanomethyl acetate; With disodium hydrogenphosphate; dihydrogen peroxide; urea; trifluoroacetic acid; In dichloromethane; at 4 ℃; for 2h; Inert atmosphere;

ethanol; With potassium carbonate; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.200804777