(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

Base Information

Chemical Name:(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester
CAS No.:233604-27-8
Molecular Formula:C₁₄H₁₄N₂O₃
Molecular Weight:258.277
Hs Code.:

Synonyms:(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

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Technology Process of (E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

There total 1 articles about (E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67-56-1
methanol

: 233604-29-0
(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid

: 233604-27-8
(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

Guidance literature:: for 0.5h;
DOI:10.1055/s-1999-3511

Reference yield: 75.0%

: 233604-27-8
(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

: 233604-29-0
(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid

Guidance literature:: With sodium hydroxide; water; In isopropyl alcohol; at 90 ℃;
DOI:10.1055/s-1999-3511

Reference yield:

: 233604-27-8
(E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid methyl ester

: (E)-3-[5-(2,5-Dimethylphenyl)-1,3,4-oxadiazol-2-yl]propenoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaOH; H₂O / propan-2-ol / 90 °C

2: PCl₃ / benzene / 14 h / 20 °C

With sodium hydroxide; water; phosphorus trichloride; In isopropyl alcohol; benzene; 1: Hydrolysis / 2: Substitution;
DOI:10.1055/s-1999-3511