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Technology Process of N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]

N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]

Base Information
  • Chemical Name:N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]
  • CAS No.:318497-16-4
  • Molecular Formula:C16H36N*C24H31Mn4N4O20
  • Molecular Weight:1157.75
  • Hs Code.:
N(C<sub>4</sub>H<sub>9</sub>)4<sup>(1+)</sup>*Mn<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CCH<sub>3</sub>)7((CHNHCHNC)CH<sub>2</sub>CO<sub>2</sub>)2<sup>(1-)</sup>=N(C<sub>4</sub>H<sub>9</sub>)4[Mn<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CCH<sub>3</sub>)7((CHNHCHNC)CH<sub>2</sub>CO<sub>2</sub>)2]

Synonyms:N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]

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Chemical Property of N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]
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Technology Process of N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]

There total 1 articles about N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

tetra-n-butylammonium permanganate
35638-41-6

tetra-n-butylammonium permanganate

imidazole-4-acetic acid hydrochloride
3251-69-2

imidazole-4-acetic acid hydrochloride

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

acetic acid
64-19-7,77671-22-8

acetic acid

N(C<sub>4</sub>H<sub>9</sub>)4<sup>(1+)</sup>*Mn<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CCH<sub>3</sub>)7((CHNHCHNC)CH<sub>2</sub>CO<sub>2</sub>)2<sup>(1-)</sup>=N(C<sub>4</sub>H<sub>9</sub>)4[Mn<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CCH<sub>3</sub>)7((CHNHCHNC)CH<sub>2</sub>CO<sub>2</sub>)2]
318497-16-4

N(C4H9)4(1+)*Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2(1-)=N(C4H9)4[Mn4O2(O2CCH3)7((CHNHCHNC)CH2CO2)2]

Guidance literature:
In methanol; acetonitrile; to a stirred soln. of Mn(O2CMe)2 and CH3COOH in MeCN N(C4H9)4MnO4 slowlyadded in small portions, mixt. of soln. of (CHNHCHNHClCCH2CO2H) in MeCN and N(C4H9)4OH in MeOH added, mixt. stirred overnight; ppt. filtered, soln. evapd., Et2O added, ppt. recrystd. from MeCN-Et2O, dried (vac.); detnd. by elem. anal.;
DOI:10.1016/S0277-5387(00)00516-7
upstream raw materials:

tetra-n-butylammonium permanganate

imidazole-4-acetic acid hydrochloride

manganese (II) acetate tetrahydrate

acetic acid

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