ethyl 1-phenylpentyl sulfide

Base Information

Chemical Name:ethyl 1-phenylpentyl sulfide
CAS No.:134895-07-1
Molecular Formula:C₁₃H₂₀S
Molecular Weight:208.368
Hs Code.:

Synonyms:ethyl 1-phenylpentyl sulfide

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Chemical Property of ethyl 1-phenylpentyl sulfide

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Technology Process of ethyl 1-phenylpentyl sulfide

There total 2 articles about ethyl 1-phenylpentyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 109-72-8,29786-93-4
n-butyllithium

: 99180-11-7
2-<(ethylthio)methyl>bromobenzene

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 134754-73-7
9-{2-(ethylthiomethyl)phenyl}-9-borabicyclo{3.3.1}nonane

: 134754-74-8,145680-12-2,134780-91-9
9-{2-(1-ethylthiopentyl)phenyl}-9-borabicyclo{3.3.1}nonane

: 6263-62-3
benzyl(ethyl)sulfane

: 134895-07-1
ethyl 1-phenylpentyl sulfide

Guidance literature:: With methanesulfonic acid; In tetrahydrofuran; diethyl ether; hexane; hexane soln. of BuLi added to an ether soln. of bromide under N2 at -30°C, at 0°C THF soln. of 9-BBN added during 1 min, immediately MsOH added at 0°C, mixture was stirred for 1 h at room temp.; filtered, filtrate evapd., residue chromd. on SiO2, ethylthiomethyl B-deriv. purified by HLPC (hexane) and recrystd. from hexane-ether (elem. anal.), 1-ethylthiopentyl B-deriv. recrystd. from hexane (elem. anal.);
DOI:10.1246/bcsj.64.1563