1,1'-Ethylenebis(3-methylpiperidine)

Base Information

Chemical Name:1,1'-Ethylenebis(3-methylpiperidine)
CAS No.:67990-20-9
Molecular Formula:C14H28N2
Molecular Weight:224.3855
Hs Code.:
European Community (EC) Number:268-042-4
DSSTox Substance ID:DTXSID60887091
Nikkaji Number:J287.772D
Mol file:67990-20-9.mol

Synonyms:1,1'-Ethylenebis(3-methylpiperidine);67990-20-9;1,1'-ETHYLENEBIS[3-METHYLPIPERIDINE];EINECS 268-042-4;Piperidine, 1,1'-(1,2-ethanediyl)bis[3-methyl-;Piperidine, 1,1'-(1,2-ethanediyl)bis(3-methyl-;DTXSID60887091

Suppliers and Price of 1,1'-Ethylenebis(3-methylpiperidine)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,1'-Ethylenebis(3-methylpiperidine)

Chemical Property:

Boiling Point:278.6°Cat760mmHg
Flash Point:111.3°C
PSA：6.48000
Density:0.902g/cm³
LogP:2.32600
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:224.225248902
Heavy Atom Count:16
Complexity:183

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCCN(C1)CCN2CCCC(C2)C

Technology Process of 1,1'-Ethylenebis(3-methylpiperidine)

There total 2 articles about 1,1'-Ethylenebis(3-methylpiperidine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 106-93-4
ethylene dibromide

: 626-56-2,53152-98-0
3-Methylpiperidine

: 67990-20-9
1,2-bis(3-methylpiperidin-1-yl)ethane

Guidance literature:: for 6h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.056

Reference yield: 70.0%

: 124-38-9,18923-20-1
carbon dioxide

: 626-56-2,53152-98-0
3-Methylpiperidine

: 67990-20-9
1,2-bis(3-methylpiperidin-1-yl)ethane

Guidance literature:: With 5 wt% Pd/C; hydrogen; 1-butyl-3-methylimidazolium chloride; 1-butyl-3-methylimidazolium Tetrafluoroborate; for 12h; under 60006 Torr; Autoclave; Heating;
DOI:10.1039/c9sc03242h