2,5-dimethylphenyl methanesulfonate

Base Information

Chemical Name:2,5-dimethylphenyl methanesulfonate
CAS No.:496837-65-1
Molecular Formula:C₉H₁₂O₃S
Molecular Weight:200.258
Hs Code.:
Mol file:496837-65-1.mol

Synonyms:2,5-dimethylphenyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-dimethylphenyl methanesulfonate

Chemical Property:

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Technology Process of 2,5-dimethylphenyl methanesulfonate

There total 2 articles about 2,5-dimethylphenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 95-87-4
2,5-Dimethylphenol

: 124-63-0
methanesulfonyl chloride

: 496837-65-1
2,5-dimethylphenyl methanesulfonate

Guidance literature:: With triethylamine; In ethyl acetate; at 0 - 20 ℃; for 0.166667h; Green chemistry;
DOI:10.1055/s-0034-1378867

Reference yield:

: 106-42-3
para-xylene

: 496837-65-1
2,5-dimethylphenyl methanesulfonate

Guidance literature:: With bis(methanesulfonyl)peroxide; at 23 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.8b09208

Reference yield: 80.0%

: 496837-65-1
2,5-dimethylphenyl methanesulfonate

: 124-40-3
dimethyl amine

: 17327-77-4
N,N,2,5-tetramethylaniline

Guidance literature:: With potassium phosphate; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; In 1,4-dioxane; tert-butyl alcohol; at 110 ℃; chemoselective reaction; Inert atmosphere; Glovebox;
DOI:10.1002/anie.201303305