C₂₅H₂₉F₆NO₄

Base Information

Chemical Name:C₂₅H₂₉F₆NO₄
CAS No.:1313494-66-4
Molecular Formula:C₂₅H₂₉F₆NO₄
Molecular Weight:521.5
Hs Code.:

C<sub>25</sub>H<sub>29</sub>F<sub>6</sub>NO<sub>4</sub>

Synonyms:C₂₅H₂₉F₆NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₉F₆NO₄

Chemical Property:

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Technology Process of C₂₅H₂₉F₆NO₄

There total 5 articles about C₂₅H₂₉F₆NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1291083-50-5
tert-butyl (1R,2R)-2-(3,5-bis(trifluoromethyl)benzyloxy)-5-(tert-butyldimethylsilyloxy)-1-phenylpentylcarbamate

: 1313494-66-4
C₂₅H₂₉F₆NO₄

Guidance literature:: tert-butyl (1R,2R)-2-(3,5-bis(trifluoromethyl)benzyloxy)-5-(tert-butyldimethylsilyloxy)-1-phenylpentylcarbamate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; Inert atmosphere;
DOI:10.1016/j.tet.2011.02.031

Reference yield:

: 1291083-49-2
tert-butyl (1R,2R)-5-(tert-butyldimethylsilyloxy)-2-hydroxy-1-phenylpentylcarbamate

: 1313494-66-4
C₂₅H₂₉F₆NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.58 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

With tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2011.02.031

Reference yield:

: 1291083-48-1
(R)-(-)-tert-butyl 5-(tert-butyldimethylsilyloxy)-2-oxo-1-phenylpentylcarbamate

: 1313494-66-4
C₂₅H₂₉F₆NO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / ethanol; dichloromethane / 7 h / -78 - -40 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.58 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

With sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2011.02.031