Diphenyl phenylphosphoramidate

Base Information

• Chemical Name: Diphenyl phenylphosphoramidate
• CAS No.: 3848-51-9
• Molecular Formula: C18H16 N O3 P
• Molecular Weight: 325.304
• Hs Code.: 2931900090
• European Community (EC) Number: 667-804-7
• DSSTox Substance ID: DTXSID30191798
• Nikkaji Number: J111.617G
• Wikidata: Q83064376
• ChEMBL ID: CHEMBL1368844
• Mol file: 3848-51-9.mol

Synonyms:Diphenyl phenylphosphoramidate;3848-51-9;Diphenyl anilinophosphonate;N-diphenoxyphosphorylaniline;Diphenyl anilidophosphate;Phenylphosphoramidic acid diphenyl ester;PHOSPHORAMIDIC ACID, PHENYL-, DIPHENYL ESTER;BRN 2148196;S 757;4-12-00-01084 (Beilstein Handbook Reference);Diphenylphenylphosphoramidate;Diphenyl phenylamidophosphate;MLS001049374;Diphenyl phenylamidophosphate #;C18H16NO3P;Diphenyl N-phenylphosphoramidate;SCHEMBL7734146;CHEMBL1368844;DTXSID30191798;HMS2786M12;C18-H16-N-O3-P;BBL018841;MFCD00091511;STK046011;AKOS001023645;N-Phenylphosporamidic acid diphenyl ester;NCGC00246381-01;Phenyl-phosphoramidic acid diphenyl ester;SMR000427319;LS-107358;CS-0368213;FT-0743271;Z56757337

Chemical Property of Diphenyl phenylphosphoramidate

Chemical Property:

• Vapor Pressure: 6.66E-08mmHg at 25°C
• Boiling Point: 438.9°Cat760mmHg
• Flash Point: 219.2°C
• PSA: 57.37000
• Density: 1.284g/cm³
• LogP: 5.43760
• XLogP3: 5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 325.08678037
• Heavy Atom Count: 23
• Complexity: 362

Purity/Quality:

98%,99%, ^*data from raw suppliers

DIPHENYL ANILINOPHOSPHONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NP(=O)(OC2=CC=CC=C2)OC3=CC=CC=C3

Technology Process of Diphenyl phenylphosphoramidate

There total 18 articles about Diphenyl phenylphosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.1%

aniline (62-53-3) + chlorophosphoric acid diphenyl ester (2524-64-3) → phenyl-amidophosphoric acid diphenyl ester (3848-51-9)

Guidance literature:

With water; In acetonitrile; at 25 ℃; Rate constant;

Reference yield: 67.0%

diphenyl hydrogen phosphite (4712-55-4) + aniline (62-53-3) → phenyl-amidophosphoric acid diphenyl ester (3848-51-9)

Guidance literature:

With tetrachloromethane; tetrabutylammomium bromide; potassium carbonate; In dichloromethane; at 0 - 20 ℃; for 4h;

DOI:10.1080/10426500500536614

Reference yield:

aniline (62-53-3) + phenol (108-95-2,27073-41-2) → phenyl (N,N'-phenyl)phosphorodiamidate (18995-02-3) + phenyl-amidophosphoric acid diphenyl ester (3848-51-9)

Guidance literature:

phenol; With magnesium chloride; trichlorophosphate; In 1,2-dichloro-ethane; at 70 - 100 ℃; for 2h;

aniline; With triethylamine; In dichloromethane; 1,2-dichloro-ethane; at 30 - 70 ℃; for 2h; Overall yield = 76.55 %; Overall yield = 48.54 g;

upstream raw materials:

triphenyl phosphite

2,4-dichloro-1,3-diphenyl-cyclodiphosphazane-2,4-dioxide

sodium phenoxide

phenyl-imidophosphoric acid triphenyl ester

Downstream raw materials:

aniline

phenol

Diphenyl-N-chlor-N-phenylphosphoramidat

dimethyl N-phenyl-phosphoramidate