2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

Base Information

Chemical Name:2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol
CAS No.:1307741-27-0
Molecular Formula:C₁₅H₁₉F₆NO₃
Molecular Weight:375.311
Hs Code.:

Synonyms:2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

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Technology Process of 2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

There total 1 articles about 2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 356537-67-2
2,5-dimethoxy-N-butylaniline

: 684-16-2
Hexafluoroacetone

: 1307741-27-0
2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 120 ℃; for 10h;
DOI:10.1016/j.bmc.2011.03.002

Reference yield: 78.0%

: 609-67-6
2-Iodobenzoyl chloride

: 1307741-27-0
2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

: 1307741-41-8
N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2,5-dimethoxyphenyl]-2-iodobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2011.03.002

Reference yield: 71.0%

: 1307741-27-0
2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

: 22921-68-2
2-bromo-5-methoxy-benzoic acid

: 1307741-45-2
2-bromo-N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2,5-dimethoxyphenyl]-5-methoxybenzamide

Guidance literature:: 2-bromo-5-methoxy-benzoic acid; With Vilsmeier reagent; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

2-(4-butylamino-2,5-dimethoxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol; With triethylamine; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.002