C₁₅H₁₈INO₅

Base Information Edit

Chemical Name:C₁₅H₁₈INO₅
CAS No.:874347-52-1
Molecular Formula:C₁₅H₁₈INO₅
Molecular Weight:419.216
Hs Code.:
Mol file:874347-52-1.mol

C<sub>15</sub>H<sub>18</sub>INO<sub>5</sub>

Synonyms:C₁₅H₁₈INO₅

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Chemical Property of C₁₅H₁₈INO₅ Edit

Chemical Property:

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Technology Process of C₁₅H₁₈INO₅

There total 6 articles about C₁₅H₁₈INO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23602-64-4
2-hydroxy-3-iodo-benzaldehyde

: 874347-52-1
C₁₅H₁₈INO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 24 h / 0 - 20 °C

2.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9

3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

3.2: pH 7 / Alkaline aqueous solution

4.1: benzene / Heating / reflux

5.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

5.2: 2 h

6.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; sodium hydride; sodium cyanoborohydride; pyridine hydrogenfluoride; In tetrahydrofuran; pyridine; methanol; water; N,N-dimethyl-formamide; toluene; benzene;

Reference yield:

: 874347-49-6
3-iodo-2-methoxy-benzaldehyde

: 874347-52-1
C₁₅H₁₈INO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

2.2: pH 7 / Alkaline aqueous solution

3.1: benzene / Heating / reflux

4.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

4.2: 2 h

5.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; pyridine hydrogenfluoride; In tetrahydrofuran; pyridine; methanol; water; toluene; benzene;

Reference yield:

: 874347-50-9
C₈H₁₀INO₂

: 874347-52-1
C₁₅H₁₈INO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 2 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

With titanium(IV) isopropylate; pyridine hydrogenfluoride; In tetrahydrofuran; pyridine; toluene; benzene;