Technology Process of C24H21N5O4S
There total 5 articles about C24H21N5O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; copper(l) iodide; L-proline;
In
water; dimethyl sulfoxide;
at 180 ℃;
for 0.416667h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / isopropyl alcohol / 12 h / Heating / reflux
2: hydrogenchloride; tin(ll) chloride / water; ethyl acetate / 1.67 h / 0 - 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C
4: sodium hydroxide; copper(l) iodide; L-proline / water; dimethyl sulfoxide / 0.42 h / 180 °C / Microwave irradiation
With
hydrogenchloride; sodium hydroxide; copper(l) iodide; N-ethyl-N,N-diisopropylamine; HATU; L-proline; tin(ll) chloride;
In
water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: nitric acid / water; butan-1-ol / 25 h / Heating / reflux
2: sodium hydroxide / isopropyl alcohol / 12 h / Heating / reflux
3: hydrogenchloride; tin(ll) chloride / water; ethyl acetate / 1.67 h / 0 - 20 °C
4: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C
5: sodium hydroxide; copper(l) iodide; L-proline / water; dimethyl sulfoxide / 0.42 h / 180 °C / Microwave irradiation
With
hydrogenchloride; sodium hydroxide; copper(l) iodide; nitric acid; N-ethyl-N,N-diisopropylamine; HATU; L-proline; tin(ll) chloride;
In
water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; butan-1-ol;