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(2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate

Base Information
  • Chemical Name:(2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate
  • CAS No.:1338481-41-6
  • Molecular Formula:C25H35NO4
  • Molecular Weight:413.557
  • Hs Code.:
(2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate

Synonyms:(2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate

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Chemical Property of (2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate
Chemical Property:
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Technology Process of (2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate

There total 7 articles about (2R,3R,4R)-2-(N-methyl-N-((R)-1-phenylethyl)amino)-3-(benzyloxy)-6-hydroxy-4-methylhexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.08.048
Guidance literature:
Multi-step reaction with 6 steps
1.1: water; sodium hydroxide / toluene / 0.33 h / -78 - 0 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere
2.2: 3 h / 0 - 20 °C / Inert atmosphere
3.1: acetonitrile / 0.17 h / 20 °C / Inert atmosphere
4.1: acetonitrile / 1 h / 20 °C / Inert atmosphere
5.1: Wilkinson's catalyst / tetrahydrofuran / 1.02 h / 0 °C / Inert atmosphere
6.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C / Inert atmosphere
With Wilkinson's catalyst; water; dihydrogen peroxide; sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; water; toluene; acetonitrile; mineral oil;
DOI:10.1016/j.tetlet.2011.08.048
Guidance literature:
Multi-step reaction with 2 steps
1: Wilkinson's catalyst / tetrahydrofuran / 1.02 h / 0 °C / Inert atmosphere
2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C / Inert atmosphere
With Wilkinson's catalyst; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetlet.2011.08.048
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