(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

Base Information

Chemical Name:(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol
CAS No.:1338481-37-0
Molecular Formula:C₁₅H₂₁NO
Molecular Weight:231.338
Hs Code.:

Synonyms:(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

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Chemical Property of (1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

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Technology Process of (1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

There total 2 articles about (1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₆BNO₇

: 1338481-37-0
(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

Guidance literature:: With water; sodium hydroxide; In toluene; at -78 - 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.08.048

Reference yield:

: [1'(R)-α-methylbenzyl]aziridine-2(R)-carboxaldehyde

: 1338481-37-0
(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 3.5 h / -78 °C / Inert atmosphere; Molecular sieve

2: water; sodium hydroxide / toluene / 0.33 h / -78 - 0 °C / Inert atmosphere

With water; sodium hydroxide; In toluene;
DOI:10.1016/j.tetlet.2011.08.048

Reference yield: 88.0%

: 1338481-37-0
(1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol

: 100-39-0
benzyl bromide

: 1338481-38-1
(R)-2-((1R,2R)-1-(benzyloxy)-2-methylbut-3-en-1-yl)-1-((R)-1-phenylethyl)aziridine

Guidance literature:: (1R,2R)-2-methyl-1-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)but-3-en-1-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.08.048