methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

Base Information

Chemical Name:methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate
CAS No.:1422387-15-2
Molecular Formula:C₂₁H₂₈N₄O₃S
Molecular Weight:416.544
Hs Code.:

Synonyms:methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

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Chemical Property of methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

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Technology Process of methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

There total 4 articles about methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422387-14-1
(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

: 79-22-1
methyl chloroformate

: 1422387-15-2
methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

Guidance literature:: With pyridine; In dichloromethane; at -78 ℃; for 2h;

Reference yield:

: 1329166-69-9
2‐(5,5‐dimethyl‐1,3,2‐dioxaborinan‐2‐yl)‐5‐nitroaniline

: 1422387-15-2
methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

2: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

3: pyridine / dichloromethane / 2 h / -78 °C

With pyridine; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium chloride; zinc; In methanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 10403-47-1
2-bromo 5-nitroaniline

: 1422387-15-2
methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 4.5 h / 80 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

3: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

4: pyridine / dichloromethane / 2 h / -78 °C

With pyridine; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; ammonium chloride; zinc; In methanol; dichloromethane; water; dimethyl sulfoxide;