methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate

Base Information

• Chemical Name: methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate
• CAS No.: 1189152-68-8
• Molecular Formula: C₂₄H₂₄N₂O₂S
• Molecular Weight: 404.533

Synonyms:methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate

Chemical Property of methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate

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Technology Process of methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate

There total 1 articles about methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

13-cyclohexyl-6-oxo-6,7-dihydro-5H-benzo[5,6][1,4]diazepino[7,1-a]indole-10-carboxylic acid methyl ester (863566-97-6) → methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate (1189152-68-8)

Guidance literature:

With tetraphosphorus decasulfide; sodium hydrogencarbonate; In 1,4-dioxane; at 100 ℃; for 1h;

Reference yield: 45.0%

methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate (1189152-68-8) + formic acid hydrazide (624-84-0) → methyl 10-cyclohexyl-4H-indolo[1,2-d][1,2,4]triazolo[4,3-a][1,4]benzodiazepine-7-carboxylate (1189152-69-9)

Guidance literature:

In butan-1-ol; at 140 ℃; for 2h; microwave irradiation;

Reference yield: 44.0%

methyl 13-cyclohexyl-5H-indolo[1,2-d][1,4]benzodiazepine-6(7H)-thione-10-carboxylate (1189152-68-8) + acetic acid hydrazide (1068-57-1) → methyl 10-cyclohexyl-1-methyl-4H-indolo[1,2-d][1,2,4]triazolo[4,3-a][1,4]benzodiazepine-7-carboxylate (1189152-70-2)

Guidance literature:

In butan-1-ol; at 140 ℃; for 2h; microwave irradiation;

upstream raw materials:

13-cyclohexyl-6-oxo-6,7-dihydro-5H-benzo[5,6][1,4]diazepino[7,1-a]indole-10-carboxylic acid methyl ester

Downstream raw materials:

methyl 10-cyclohexyl-1-methyl-4H-indolo[1,2-d][1,2,4]triazolo[4,3-a][1,4]benzodiazepine-7-carboxylate

methyl 10-cyclohexyl-4H-indolo[1,2-d][1,2,4]triazolo[4,3-a][1,4]benzodiazepine-7-carboxylate

methyl 10-cyclohexyl-4H-imidazo[1,2-a]indolo[1,2-d][1,4]benzodiazepine-7-carboxylate

methyl 10-cyclohexyl-2-methyl-4H-imidazo[1,2-a]indolo[1,2-d][1,4]benzodiazepine-7-carboxylate

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