11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

Base Information

Chemical Name:11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one
CAS No.:1426333-96-1
Molecular Formula:C₃₂H₂₇N₇O₂S
Molecular Weight:573.678
Hs Code.:

11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

Synonyms:11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

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Chemical Property of 11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

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Technology Process of 11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

There total 7 articles about 11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1426333-89-2
11-ethyl-8-methyl-6,9-diphenyl-10-oxo-4,5,9,11-tetrahydropyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridin-3(2H)-thione

: 70-11-1
α-bromoacetophenone

: 1426333-96-1
11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

Guidance literature:: With sodium acetate; In ethanol;
DOI:10.3390/molecules171214464

Reference yield:

: 100-52-7
benzaldehyde

: 1426333-96-1
11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / water / 1 h / 100 °C

2: sodium hydroxide / ethanol / 4 h / Reflux

3: ethanol / 12 h / Reflux

4: sodium hydroxide / ethanol / 2 h

5: sodium acetate / ethanol

With sodium acetate; toluene-4-sulfonic acid; sodium hydroxide; In ethanol; water;
DOI:10.3390/molecules171214464

Reference yield:

: 1131-18-6
1-Phenyl-3-methyl-5-aminopyrazole

: 1426333-96-1
11-ethyl-3-(2-oxo-2-phenylethylthio)-8-methyl-6,9-dipheny-10-oxo-4,5,9,11-tetrahydro-pyrazolo[5,4-b]1,2,4-triazolo[4',3'-2,1]pyrimidino[5,6-e]pyridine-10-one

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / 10 h / 100 °C

2: sodium hydroxide / ethanol / 4 h / Reflux

3: ethanol / 12 h / Reflux

4: sodium hydroxide / ethanol / 2 h

5: sodium acetate / ethanol

With sodium acetate; toluene-4-sulfonic acid; sodium hydroxide; In ethanol;
DOI:10.3390/molecules171214464