(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

Base Information

Chemical Name:(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide
CAS No.:1597531-42-4
Molecular Formula:C₂₃H₂₁F₃N₆O₄
Molecular Weight:502.453
Hs Code.:

Synonyms:(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

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Chemical Property of (S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

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Technology Process of (S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

There total 4 articles about (S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1979-29-9
2-(trifluoromethoxy)benzoic acid

: 1597528-83-0
(S)-N-hydroxy-1-(5-methyl-2-[1,2,3]triazol-2-yl-benzoyl)pyrrolidine-2-carboxamidine

: 1597531-42-4
(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1597528-77-2
(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)pyrrolidine-2-carbonitrile

: 1597531-42-4
(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 1 h / 20 °C

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With hydroxylamine hydrochloride; sodium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

Reference yield:

: 204387-53-1
(2S)-pyrrolidine-2-carbonitrile

: 1597531-42-4
(S)-1-(5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl)-N-((2-(trifluromethoxy)benzoyl)oxy)pyrrolidine-2-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 1 h / 20 °C

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With hydroxylamine hydrochloride; sodium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;