1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

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Chemical Name:1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose
CAS No.:308279-01-8
Molecular Formula:C₃₀H₃₀O₅
Molecular Weight:470.565
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

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Chemical Property of 1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

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Technology Process of 1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

There total 1 articles about 1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 262300-87-8
1,2-O-isopropylidene-3-O-propargyl-5-O-trityl-α-D-xylofuranose

: 308279-01-8
1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; tert-butyl alcohol; at 55 ℃; for 1h;
DOI:10.1016/S0957-4166(00)00260-3

Reference yield: 77.0%

: 75-77-4
chloro-trimethyl-silane

: 308279-01-8
1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

: 1,2-O-isopropylidene-3-O-(1'-trimethylsilylpropa-1',2'-dienyl)-5-O-trityl-α-D-xylo-furanose

Guidance literature:: 1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose; With n-butyllithium; In tetrahydrofuran; hexane; at -30 ℃; for 0.5h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -30 - 20 ℃; for 0.75h;
DOI:10.1016/S0957-4166(00)00260-3

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 308279-01-8
1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose

: (4'S)-1,2-O-isopropylidene-3-O-(3'-methyleneazetidin-2'-on-4'-yl)-5-O-trityl-α-D-xylofuranose

: (4'R)-1,2-O-isopropylidene-3-O-(3'-methyleneazetidin-2'-on-4'-yl)-5-O-trityl-α-D-xylofuranose

Guidance literature:: isocyanate de chlorosulfonyle; 1,2-O-isopropylidene-3-O-(prop-1',2'-dienyl)-5-O-trityl-α-D-xylofuranose; With sodium carbonate; In toluene; at -70 - -30 ℃; for 1.5h;

With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; at -70 - 0 ℃; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(00)00260-3