Technology Process of C25H14BrClF10N2O3
There total 6 articles about C25H14BrClF10N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
toluene;
at 80 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Reflux
2.1: pyridine / tetrahydrofuran / 6 h / 20 °C / Reflux
3.1: potassium carbonate / 16 h / 20 °C
4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C
4.2: pH 7 - 8
5.1: N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
With
pyridine; hydrogenchloride; oxalyl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride;
N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; water; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 1 h / 100 °C
2.1: pyridine / tetrahydrofuran / 18 h / 20 °C / Reflux
2.2: 41 h / 20 °C
3.1: potassium carbonate / 16 h / 20 °C
4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C
4.2: pH 7 - 8
5.1: N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
With
pyridine; hydrogenchloride; thionyl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride;
N,N-dimethyl-formamide;
In
tetrahydrofuran; water; isopropyl alcohol; toluene;