4-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]phenyl methyl ether

Base Information

• Chemical Name: 4-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]phenyl methyl ether
• CAS No.: 93986-11-9
• Molecular Formula: C₁₅H₁₁ClN₂O₂
• Molecular Weight: 286.718
• Mol file: 93986-11-9.mol

Synonyms:2-(4-chlorophenyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole

Chemical Property of 4-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]phenyl methyl ether

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-(4-chlorophenyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 4-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]phenyl methyl ether

There total 17 articles about 4-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]phenyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C15H13ClN2O2 (51771-22-3) → 2-(4-chlorophenyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole (93986-11-9)

Guidance literature:

With oxygen; copper(II) bis(trifluoromethanesulfonate); caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 10h;

DOI:10.1021/ol202409r

Reference yield: 87.0%

4-Chloro-benzoic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide (51771-28-9) → 2-(4-chlorophenyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole (93986-11-9)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1016/j.tetlet.2009.02.054

Reference yield: 87.0%

4-methoxy-benzoyl chloride (100-07-2) + 5-(4-chlorophenyl)tetrazole (16687-61-9) → 2-(4-chlorophenyl)-5-(4-methoxyphenyl)-1,3,4-oxadiazole (93986-11-9)

Guidance literature:

With pyridine; In toluene; for 3h; Reflux; Inert atmosphere;

DOI:10.1021/acs.jmedchem.5b01439

upstream raw materials:

4-methoxy-benzoic acid N'-(4-chloro-benzoyl)-hydrazide

4-methoxy-benzaldehyde

4-chlorobenzoic acid hydrazide

4-Chloro-benzoic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

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