4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

Base Information

Chemical Name:4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate
CAS No.:181188-34-1
Molecular Formula:C₁₂H₁₄F₅O₆PS
Molecular Weight:412.271
Hs Code.:

Synonyms:4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

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Chemical Property of 4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

There total 3 articles about 4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 109586-39-2
4-iodophenyl trifluoromethanesulfonate

: 82845-20-3
[(diethoxyphosphoryl)difluoromethyl]zinc bromide

: 181188-34-1
4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

Guidance literature:: With copper(I) bromide; In N,N-dimethyl acetamide; Irradiation;
DOI:10.1016/S0960-894X(99)00027-X

Reference yield: 66.0%

: 65094-22-6
diethyl (bromodifluoromethyl)phosphonate

: 109586-39-2
4-iodophenyl trifluoromethanesulfonate

: 181188-34-1
4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

Guidance literature:: With copper(I) bromide; zinc; for 18h; sonication;
DOI:10.1016/S0040-4039(99)00266-X

Reference yield:

: 540-38-5
p-Iodophenol

: 181188-34-1
4-[(Diethoxyphosphoryl)difluoromethyl]phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / CH₂Cl₂ / 0 °C

2: 66 percent / Zn, CuBr / 18 h / sonication

With pyridine; copper(I) bromide; zinc; In dichloromethane;
DOI:10.1016/S0040-4039(99)00266-X