2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

Base Information

Chemical Name:2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole
CAS No.:175530-95-7
Molecular Formula:C₁₇H₁₈N₄O₂
Molecular Weight:310.356
Hs Code.:

Synonyms:2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

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Chemical Property of 2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

Chemical Property:

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Technology Process of 2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

There total 3 articles about 2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.6%

: 33259-72-2
2,3-diamino-6-methyl-pyridine

: 39608-31-6
N-(Benzyloxycarbonyl)sarcosine

: 543-27-1
isobutyl chloroformate

: 175530-95-7
2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

Guidance literature:: With triethylamine; In tetrahydrofuran; methanol; glacial AcOH; ethyl acetate; toluene;

Reference yield: 46.6%

: 33259-72-2
2,3-diamino-6-methyl-pyridine

: 39608-31-6
N-(Benzyloxycarbonyl)sarcosine

: 121-44-8
triethylamine

: 543-27-1
isobutyl chloroformate

: 175530-95-7
2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

Guidance literature:: In tetrahydrofuran; methanol; glacial AcOH; ethyl acetate; toluene;

Reference yield:

: 1824-81-3
2-Amino-6-methylpyridine

: 175530-95-7
2-[[N-(Benzyloxycarbonyl)-N-methyl]aminomethyl]-5-methyl4-azabenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; Concentrated HNO₃

2: palladium-carbon / methanol

3: tetrahydrofuran; methanol; glacial AcOH; ethyl acetate; toluene

With sodium hydroxide; Concentrated HNO₃; palladium-carbon; In tetrahydrofuran; methanol; glacial AcOH; ethyl acetate; toluene;