benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

Base Information

Chemical Name:benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate
CAS No.:1470362-91-4
Molecular Formula:C₂₁H₂₅N₃O₆
Molecular Weight:415.446
Hs Code.:

Synonyms:benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

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Technology Process of benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

There total 4 articles about benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1470362-95-8
C₂₀H₂₃N₃O₆

: 74-88-4
methyl iodide

: 1470362-91-4
benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃;
DOI:10.2174/15701786113109990028

Reference yield:

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 1470362-91-4
benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 24 h

2: ethanol / 80 °C

3: potassium carbonate / acetone / 50 °C

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.2174/15701786113109990028

Reference yield:

: 26582-86-5
benzyl (1S)-2-hydrazino-1-(hydroxymethyl)-2-oxoethylcarbamate

: 1470362-91-4
benzyl (1S)-2-[(2E)-2-(2,3-dimethoxyphenyl)methylidene]-1-(hydroxymethyl)-2-oxoethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 80 °C

2: potassium carbonate / acetone / 50 °C

With potassium carbonate; In ethanol; acetone;
DOI:10.2174/15701786113109990028