phenylborane; compound with triethylamine (1:1)

Base Information

Chemical Name:phenylborane; compound with triethylamine (1:1)
CAS No.:857404-98-9
Molecular Formula:C₆H₇B*C₆H₁₅N
Molecular Weight:191.124
Hs Code.:

Synonyms:phenylborane; compound with triethylamine (1:1)

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Chemical Property of phenylborane; compound with triethylamine (1:1)

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Technology Process of phenylborane; compound with triethylamine (1:1)

There total 3 articles about phenylborane; compound with triethylamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: Cp2ZrCl((μ-H)2BHPh)2*0.5toluene

: 121-44-8
triethylamine

: 847056-82-0
Cp2ZrH((μ-H)2BHPh)

: 857404-98-9
phenylborane; compound with triethylamine (1:1)

Guidance literature:: In toluene; (drybox); addn. of toluene to zirconium complex at -78°C, addn. of amine, warming to room temp., stirring for 4 h; evapn., dissolving in Et2O, storage at -35°C, manual sepn.;
DOI:10.1016/j.jorganchem.2004.09.026

Reference yield:

: (carbonyl)4(cobalt)BH₂*THF

: 100-58-3
phenylmagnesium bromide

: 53433-12-8
[bis(triphenylphospine)nitrogen⁽¹⁺⁾][Co(CO)4]

: 960-71-4
triphenylborane

: triethylamine borane

: 857404-98-9
phenylborane; compound with triethylamine (1:1)

Guidance literature:: With Et₃N; (PPN)Cl; In tetrahydrofuran; Under N2, evapn. of volatiles from a Co-complex soln. (-20°C), addn. of fresh THF and PhMgBr, stirring (-20°C, 5 h; room temp., 2 h), addn. of Et3N, stirring overnight at room temp., metathesis with (PPN)Cl.; Monitored by (11)B-NMR, Et2O-sol. fraction yields B containing compounds.;