N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid

Base Information

• Chemical Name: N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid
• CAS No.: 906667-53-6
• Molecular Formula: C₂₃H₁₉NO₅
• Molecular Weight: 389.408
• Mol file: 906667-53-6.mol

Synonyms:N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid

Chemical Property of N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid

Chemical Property:

Purity/Quality:

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Technology Process of N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid

There total 1 articles about N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(fluorenylmethoxy)carbonyl chloride (28920-43-6) + 4-(aminooxymethyl)benzoic acid hydrochloride (20228-85-7) → N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid (906667-53-6)

Guidance literature:

With sodium carbonate; In 1,4-dioxane; for 2h;

DOI:10.1002/anie.200600642

Reference yield: 89.0%

N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid (906667-53-6) + bromoacetic acid tert-butyl ester (5292-43-3) → C29H29NO7

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h;

DOI:10.1002/anie.200600642

Reference yield:

N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid (906667-53-6) + benzyl bromide (100-39-0) → C30H25NO5

Guidance literature:

N-(fluoren-9-ylmethyloxycarbonyl)-4-(aminooxymethyl)benzoic acid; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

upstream raw materials:

(fluorenylmethoxy)carbonyl chloride

4-(aminooxymethyl)benzoic acid hydrochloride